Shimadzu BL3200S Instruction Manual Page 224
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- Table of contents
- TROUBLESHOOTING
- BOOKMARKS
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7. Hardware Validation
7-26
RF-20A/20Axs
11
Set a Chromatopac as follows.
12
Move the Chromatopac's pen position to the zero
on the recording paper, then start recording with
the Chromatopac.
13
Press .
Measurement of noise starts automatically.
During measurement, the screen to the right is
displayed.
After 15 minutes of measuring the noise, the peak
value of the raman spectrum (the value at F on the
screen to the right) and the S/N ratio are
calculated and shown on the screen.
14
This completes recording by the Chromatopac.
15
On pressing several times, the
performance inspection is ended and the initial
screen is redisplayed.
Item Set Set Value
ATTEN 1 (2 mV/full scale)
SPEED 10 mm/min
350/***nm1000.00
TIME=***s
Signal value
Remaining measuring time
S/N CHECK
F:** S/N:****
Peak value of the
raman spectrum
S/N ratio
- RF-20A/20Axs 1
- Warranty 1. Period: 4
- 2. Description: 4
- 3. Exceptions: 4
- Safety Instructions 6
- !WARNING 10
- Introduction 12
- !CAUTION 13
- Disposal Precautions 21
- Warning Labels 22
- Side of the Instrument 23
- Action for Environment (WEEE) 24
- European Union: 24
- Contents 25
- Chapter 3 Preparation 26
- Chapter 4 Basic Operation 26
- Chapter 6 Troubleshooting 31
- Chapter 7 Hardware Validation 31
- Chapter 8 Maintenance 32
- Configuration 37
- 1.1 Overview 38
- 1.2 Features 39
- 1.3 Component Parts 40
- 1.4 Optional Parts 41
- Photomultiplier for RF-20A 42
- 2.1 Front 44
- Left Side 45
- 2.3 Right Side and Base Panel 46
- 2.4 Back 47
- 2.5.1 Display Panel 48
- 2.5.2 Keypad 50
- Preparation 53
- 3.1 Cautions on Operation 54
- 3.2 Turning the Power ON/OFF 55
- 3. Preparation 56
- RF-20AXS V*.** 57
- Basic Operation 59
- ∗ : RF-20Axs only 63
- When a Recorder Is Used: 65
- EX200n m EM30 0nm 66
- X e 1000.00 66
- PARAMETER 72
- RESPON S E5 73
- Input 0 - 1 0 73
- 1:x1 2:x 43: x16 75
- Input 0 - 3,8 85
- EX200n m EM3 00nm 87
- X e:c h 1 1000.00 87
- 10.0 sec 93
- 4.2.8 Setting Sensitivity 96
- 1:HI 2:M ED 3:LOW 97
- 0:OFF, 4-40 99
- 4. Basic Operation 100
- Application Operation 101
- Types of Screen and Their 102
- Explanations 102
- 5. Application Operation 104
- Press to 105
- Control settings group 105
- Monitor display group 107
- 5.1.3 VP Function Screen 108
- Validation support group 109
- CBM PARAMETER 111
- Enter to Select 111
- CHANGE PASSWORD 111
- Enter to Change 111
- Parameter Settings Group 113
- Control Settings Group 113
- System Settings Group 114
- Monitor Display Group 114
- RESPONSE 5 118
- Input 0 - 10 118
- 1:HI 2:MED 3:LOW 119
- 1:x1 2:x4 3:x16 119
- ANALOG1 MODE 0 120
- Input 0 - 1 120
- Input 0 - 1,8 120
- ANALOG2 MODE 0 121
- ANA1 REC RANG 1 122
- Input 0 - 9 122
- ANA2 REC RANG 1 123
- BL OFS ANA1 0 124
- Input -2 - 250mV 124
- BL OFS ANA2 0 124
- 0,1,2 or 12 125
- MARK SETTING 125
- Input 0 - 3 125
- 5.2.4 Control Settings Group 126
- EM SCAN 200-900 127
- Input 200 - 900 127
- Input 0,200-900 127
- 5.2.5 System Settings Group 129
- BRIGHTNESS 3 130
- Input 1 - 4 130
- EXT-S 0 130
- Input 0 - 5 130
- SMPL EN 873 132
- REF EN 1211 132
- Xe TIME 2000.0 132
- Set temperature 133
- Current temperature 133
- 5.3 Setting the VP Functions 134
- Validation Support Group 135
- Calibration Support Group 135
- Time [Xe LAMP USED TM] 138
- ERROR LOG 140
- Enter to Display 140
- LOG 1 08-05-12 140
- ERR LEAK DETECT 140
- No more Logs 140
- Entering the Date [DATE] 141
- Entering the Time [TIME] 141
- OP MODE 0 146
- 0:20A 1:XL 146
- INITIALIZE PARAM 146
- Enter to Init 146
- [INTERFACE] 150
- ETHERNET SPEED 0 151
- Input 0, 1-4 151
- USE GATEWAY 0 151
- 0:NO 1:GW 2:DHCP 151
- TRS MODE 3 153
- Input 0, 1-19 153
- 5.4 Creating Time Programs 154
- 5.4 Creating Time Programs 155
- Setting multiple steps: 158
- 30.00 LOOP 3 159
- Input 0 - 255 159
- 5.00 SCAN 2 159
- Input 0 - 2 159
- 5.4.5 Starting a Time Program 160
- Outputting Spectrum Data 162
- 5.5.3 Setting the Scan Type 163
- EX SCAN 200-900 164
- Input 0,2 0 0-900 165
- 5.5.6 Setting the Scan Speed 166
- SCAN SPEED 2 166
- Input 1 - 4 166
- 5.5.7 Setting Sensitivity 167
- 5.5.8 Setting Gain 168
- CELL TEMP 0 169
- 0:OFF, 4 - 40 169
- EX200nm EM300nm 170
- Xe 1000.00 170
- Enter to Select 170
- SCAN FILE 0 171
- 0:BG 1:S1 2:S2 171
- 5.5.11 Measuring Procedure 172
- SPC PLOT 174
- PLOTTIING 174
- Connecting to a CBM-20A or 175
- CBM-20Alite System Controller 175
- Controller 176
- 5.7.3 Notes on Operation 177
- XL Compatibility Mode 177
- VP function 180
- Terminals 181
- 5.8.2 Wiring 182
- EVENT 1 183
- 0,1,2 or 12 183
- Optional Cell 184
- Troubleshooting 185
- 6. Troubleshooting 186
- Dealing with Error Messages 189
- ERR EX HOME POS 190
- ERR EM HOME POS 190
- ERR EEPROM WRITE 190
- SYSTEM ERROR 190
- ERR COOLER 190
- ERR HEATER 191
- ERR OVER HEAT 191
- ERR LEAK SENS 191
- ERR LEAK SENS2 191
- NOT PROTECTED 192
- ERR Xe LAMP 192
- ERR Hg LAMP 193
- CHECK NG1 193
- CHECK NG2(EX***) 193
- CHECK NG3(EM***) 193
- ERR CELL TEMP 194
- LAMP COVER OPEN 194
- ERR PELTIER FAN 194
- ERR FAN STOP 195
- CBM-20A ERROR 195
- DATA NOT EXIST 195
- NO PEAKS 1 196
- NO PEAKS 2 196
- NO PEAKS 3 196
- ERR FILE TYPE 197
- LAMP NOT LIT 197
- SENSOR NO GOOD 197
- SELECT Xe SINGLE 197
- LOW SET TEMP 198
- CLOSED KEY 198
- NO CAL DATA 198
- NOT LOCAL MODE 198
- Hardware Validation 199
- 7.1.1 Hardware Validation 200
- Implementation of Hardware 201
- Validation 201
- 7.3 Precautions on Validation 202
- Testing Equipment 203
- Hardware Testing Equipment 204
- 7.5 Detector Validation 205
- Objective 206
- Check Procedure 206
- 7. Hardware Validation 210
- 7.5 Detector Validation 211
- When LCsolution is used: 213
- VALIDATION 214
- Press func or VP 214
- DATE YY-MM-DD 214
- 00-00-00 214
- S/N CHECK 221
- Enter to Start 221
- S/N CHECK ENTER 222
- 350/***nm1000.00 224
- TIME=***s 224
- F:** S/N:**** 224
- S/N ≥ 600 (RF-20A) 225
- 1000 (RF-20Axs) 225
- 0:Remote 1:Local 226
- NO PEAK * 228
- S/N ≥ 1000 (RF-20Axs) 230
- LEAK SENSOR TEST 232
- CHECK GOOD 232
- 7.6 System Validation 233
- 7.6 System Validation 235
- EX360nm EM450nm 237
- 7.7 If Validation Fails 244
- 7.8 Reference Information 245
- 7.8 Reference Information 247
- Maintenance 251
- 8. Maintenance 254
- 8.2.1 Inspecting the Cell 255
- Inspecting the Cell 256
- Fitting the Flow Cell Unit 257
- Parts used 258
- Simple Cleaning of the Cell 259
- Cleaning/Replacing Each Part 261
- Fig. 8.14 263
- 8.3.2 Cleaning the Cell 267
- Fitting the Cell 268
- For the RF-20A: 270
- Fitting the Emission Lens 270
- Fitting the Emission Mirror 273
- Fig. 8.35 275
- Check After Assembly 277
- 8.5 Replacing the Fuse 285
- 8.6 Replacing the Filter 287
- Wavelength calibration 289
- Wavelength accuracy check 289
- For the RF-20Axs: 290
- EX or EM 295
- Wavelength 295
- WAVE CALIB 296
- 8.8 Cleaning the Exterior 298
- Technical Information 299
- 9.1 Installation 300
- Stacking Brackets 303
- 9.1 Installation 307
- Cutting SUS tubing: 307
- Cutting resin tubing: 307
- Protective Plugs 310
- Bending Tubing for Plumbing 310
- 9. Technical Information 314
- Plumbing the Cell Outlet Tube 314
- Lowest unit: 316
- Second unit from bottom: 317
- Front Cover Installation 319
- 9.1.7 Flow Line Plumbing 321
- Connecting to a Chromatopac 329
- Connecting to a Recorder 330
- 9.2 Specifications 338
- 9.2 Specifications 339
- 9.3 Maintenance Parts 340
- Flow Cell/Plumbing Parts 341
- Electrical Parts 342
- Others 342
- Mobile Phase Characteristics 346
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