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Instruction Manual
Shimadzu BL3200S Instruction Manual Page 319
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9.1 Installation
9-21
RF-20A/20Axs
9
Front Cover Installation
1
After perform
ing the plum
bing, install the front
cover by following the
removal procedure in
reverse.
2
Close the front cover
.
Fig. 9.31
Front cover
1
2
...
314
315
316
317
318
319
320
321
322
323
324
...
351
352
RF-20A/20Axs
1
Warranty 1. Period:
4
2. Description:
4
3. Exceptions:
4
Safety Instructions
6
!WARNING
10
Introduction
12
!CAUTION
13
Disposal Precautions
21
Warning Labels
22
Side of the Instrument
23
Action for Environment (WEEE)
24
European Union:
24
Contents
25
Chapter 3 Preparation
26
Chapter 4 Basic Operation
26
Chapter 6 Troubleshooting
31
Chapter 7 Hardware Validation
31
Chapter 8 Maintenance
32
Configuration
37
1.1 Overview
38
1.2 Features
39
1.3 Component Parts
40
1.4 Optional Parts
41
Photomultiplier for RF-20A
42
2.1 Front
44
Left Side
45
2.3 Right Side and Base Panel
46
2.4 Back
47
2.5.1 Display Panel
48
2.5.2 Keypad
50
Preparation
53
3.1 Cautions on Operation
54
3.2 Turning the Power ON/OFF
55
3. Preparation
56
RF-20AXS V*.**
57
Basic Operation
59
∗ : RF-20Axs only
63
When a Recorder Is Used:
65
EX200n m EM30 0nm
66
X e 1000.00
66
PARAMETER
72
RESPON S E5
73
Input 0 - 1 0
73
1:x1 2:x 43: x16
75
Input 0 - 3,8
85
EX200n m EM3 00nm
87
X e:c h 1 1000.00
87
10.0 sec
93
4.2.8 Setting Sensitivity
96
1:HI 2:M ED 3:LOW
97
0:OFF, 4-40
99
4. Basic Operation
100
Application Operation
101
Types of Screen and Their
102
Explanations
102
5. Application Operation
104
Press to
105
Control settings group
105
Monitor display group
107
5.1.3 VP Function Screen
108
Validation support group
109
CBM PARAMETER
111
Enter to Select
111
CHANGE PASSWORD
111
Enter to Change
111
Parameter Settings Group
113
Control Settings Group
113
System Settings Group
114
Monitor Display Group
114
RESPONSE 5
118
Input 0 - 10
118
1:HI 2:MED 3:LOW
119
1:x1 2:x4 3:x16
119
ANALOG1 MODE 0
120
Input 0 - 1
120
Input 0 - 1,8
120
ANALOG2 MODE 0
121
ANA1 REC RANG 1
122
Input 0 - 9
122
ANA2 REC RANG 1
123
BL OFS ANA1 0
124
Input -2 - 250mV
124
BL OFS ANA2 0
124
0,1,2 or 12
125
MARK SETTING
125
Input 0 - 3
125
5.2.4 Control Settings Group
126
EM SCAN 200-900
127
Input 200 - 900
127
Input 0,200-900
127
5.2.5 System Settings Group
129
BRIGHTNESS 3
130
Input 1 - 4
130
EXT-S 0
130
Input 0 - 5
130
SMPL EN 873
132
REF EN 1211
132
Xe TIME 2000.0
132
Set temperature
133
Current temperature
133
5.3 Setting the VP Functions
134
Validation Support Group
135
Calibration Support Group
135
Time [Xe LAMP USED TM]
138
ERROR LOG
140
Enter to Display
140
LOG 1 08-05-12
140
ERR LEAK DETECT
140
No more Logs
140
Entering the Date [DATE]
141
Entering the Time [TIME]
141
OP MODE 0
146
0:20A 1:XL
146
INITIALIZE PARAM
146
Enter to Init
146
[INTERFACE]
150
ETHERNET SPEED 0
151
Input 0, 1-4
151
USE GATEWAY 0
151
0:NO 1:GW 2:DHCP
151
TRS MODE 3
153
Input 0, 1-19
153
5.4 Creating Time Programs
154
5.4 Creating Time Programs
155
Setting multiple steps:
158
30.00 LOOP 3
159
Input 0 - 255
159
5.00 SCAN 2
159
Input 0 - 2
159
5.4.5 Starting a Time Program
160
Outputting Spectrum Data
162
5.5.3 Setting the Scan Type
163
EX SCAN 200-900
164
Input 0,2 0 0-900
165
5.5.6 Setting the Scan Speed
166
SCAN SPEED 2
166
Input 1 - 4
166
5.5.7 Setting Sensitivity
167
5.5.8 Setting Gain
168
CELL TEMP 0
169
0:OFF, 4 - 40
169
EX200nm EM300nm
170
Xe 1000.00
170
Enter to Select
170
SCAN FILE 0
171
0:BG 1:S1 2:S2
171
5.5.11 Measuring Procedure
172
SPC PLOT
174
PLOTTIING
174
Connecting to a CBM-20A or
175
CBM-20Alite System Controller
175
Controller
176
5.7.3 Notes on Operation
177
XL Compatibility Mode
177
VP function
180
Terminals
181
5.8.2 Wiring
182
EVENT 1
183
0,1,2 or 12
183
Optional Cell
184
Troubleshooting
185
6. Troubleshooting
186
Dealing with Error Messages
189
ERR EX HOME POS
190
ERR EM HOME POS
190
ERR EEPROM WRITE
190
SYSTEM ERROR
190
ERR COOLER
190
ERR HEATER
191
ERR OVER HEAT
191
ERR LEAK SENS
191
ERR LEAK SENS2
191
NOT PROTECTED
192
ERR Xe LAMP
192
ERR Hg LAMP
193
CHECK NG1
193
CHECK NG2(EX***)
193
CHECK NG3(EM***)
193
ERR CELL TEMP
194
LAMP COVER OPEN
194
ERR PELTIER FAN
194
ERR FAN STOP
195
CBM-20A ERROR
195
DATA NOT EXIST
195
NO PEAKS 1
196
NO PEAKS 2
196
NO PEAKS 3
196
ERR FILE TYPE
197
LAMP NOT LIT
197
SENSOR NO GOOD
197
SELECT Xe SINGLE
197
LOW SET TEMP
198
CLOSED KEY
198
NO CAL DATA
198
NOT LOCAL MODE
198
Hardware Validation
199
7.1.1 Hardware Validation
200
Implementation of Hardware
201
Validation
201
7.3 Precautions on Validation
202
Testing Equipment
203
Hardware Testing Equipment
204
7.5 Detector Validation
205
Objective
206
Check Procedure
206
7. Hardware Validation
210
7.5 Detector Validation
211
When LCsolution is used:
213
VALIDATION
214
Press func or VP
214
DATE YY-MM-DD
214
00-00-00
214
S/N CHECK
221
Enter to Start
221
S/N CHECK ENTER
222
350/***nm1000.00
224
TIME=***s
224
F:** S/N:****
224
S/N ≥ 600 (RF-20A)
225
1000 (RF-20Axs)
225
0:Remote 1:Local
226
NO PEAK *
228
S/N ≥ 1000 (RF-20Axs)
230
LEAK SENSOR TEST
232
CHECK GOOD
232
7.6 System Validation
233
7.6 System Validation
235
EX360nm EM450nm
237
7.7 If Validation Fails
244
7.8 Reference Information
245
7.8 Reference Information
247
Maintenance
251
8. Maintenance
254
8.2.1 Inspecting the Cell
255
Inspecting the Cell
256
Fitting the Flow Cell Unit
257
Parts used
258
Simple Cleaning of the Cell
259
Cleaning/Replacing Each Part
261
Fig. 8.14
263
8.3.2 Cleaning the Cell
267
Fitting the Cell
268
For the RF-20A:
270
Fitting the Emission Lens
270
Fitting the Emission Mirror
273
Fig. 8.35
275
Check After Assembly
277
8.5 Replacing the Fuse
285
8.6 Replacing the Filter
287
Wavelength calibration
289
Wavelength accuracy check
289
For the RF-20Axs:
290
EX or EM
295
Wavelength
295
WAVE CALIB
296
8.8 Cleaning the Exterior
298
Technical Information
299
9.1 Installation
300
Stacking Brackets
303
9.1 Installation
307
Cutting SUS tubing:
307
Cutting resin tubing:
307
Protective Plugs
310
Bending Tubing for Plumbing
310
9. Technical Information
314
Plumbing the Cell Outlet Tube
314
Lowest unit:
316
Second unit from bottom:
317
Front Cover Installation
319
9.1.7 Flow Line Plumbing
321
Connecting to a Chromatopac
329
Connecting to a Recorder
330
9.2 Specifications
338
9.2 Specifications
339
9.3 Maintenance Parts
340
Flow Cell/Plumbing Parts
341
Electrical Parts
342
Others
342
Mobile Phase Characteristics
346
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