Shimadzu BL3200S Instruction Manual Page 32
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Contents
Contents-8
RF-20A/20Axs
7.5.5 Checking Wavelength Accuracy ................................................................... 7-11
Objective .................................................................................................................7-11
Check Procedure (for RF-20Axs) ............................................................................7-12
Check Procedure (for RF-20A) ................................................................................7-16
7.5.6 Inspecting a Performance Using the Raman Spectrum of Water ................. 7-21
Objective .................................................................................................................7-21
Substituting Water in the Flow Line .........................................................................7-21
Check Procedure (When Using a Chromatopac) ....................................................7-23
Check Procedure (When Using LCsolution) ............................................................7-28
7.5.7 Checking the Leak Sensor ............................................................................ 7-33
Objective .................................................................................................................7-33
Check Procedure .....................................................................................................7-33
7.6 System Validation ..........................................................................................7-35
7.6.1 Validation of an Isocratic LC System ............................................................ 7-36
Objective .................................................................................................................7-36
Equipment Required for Validation ..........................................................................7-36
Checking and Preparing the LC System .................................................................7-37
Check Procedure .....................................................................................................7-38
Parameter Settings for Isocratic System Validation ................................................7-40
7.6.2 Validation of a Gradient LC System .............................................................. 7-41
Objective .................................................................................................................7-41
Equipment Required for Validation ..........................................................................7-41
Checking and Preparing the LC System .................................................................7-42
Check Procedure .....................................................................................................7-43
Parameter Settings for Isocratic System Validation ................................................7-45
7.7 If Validation Fails ............................................................................................7-46
7.8 Reference Information ....................................................................................7-47
7.8.1 Automatic Wavelength Calibration Function ................................................. 7-47
Wavelength Calibration ...........................................................................................7-47
7.8.2 Automatic Checking Function of Wavelength Accuracy ................................ 7-52
Chapter 8 Maintenance
8.1 Periodic Inspection and Maintenance ..............................................................8-2
8.1.1 Prior to Inspection and Maintenance ............................................................... 8-2
8.1.2 List of Periodic Inspection and Maintenance ................................................... 8-2
8.1.3 Check After Inspection and Maintenance ....................................................... 8-4
8.2 Inspection and Simple Washing of the Cell ......................................................8-5
8.2.1 Inspecting the Cell ........................................................................................... 8-5
Nomenclature of Flow Cell Unit Parts ........................................................................8-5
- RF-20A/20Axs 1
- Warranty 1. Period: 4
- 2. Description: 4
- 3. Exceptions: 4
- Safety Instructions 6
- !WARNING 10
- Introduction 12
- !CAUTION 13
- Disposal Precautions 21
- Warning Labels 22
- Side of the Instrument 23
- Action for Environment (WEEE) 24
- European Union: 24
- Contents 25
- Chapter 3 Preparation 26
- Chapter 4 Basic Operation 26
- Chapter 6 Troubleshooting 31
- Chapter 7 Hardware Validation 31
- Chapter 8 Maintenance 32
- Configuration 37
- 1.1 Overview 38
- 1.2 Features 39
- 1.3 Component Parts 40
- 1.4 Optional Parts 41
- Photomultiplier for RF-20A 42
- 2.1 Front 44
- Left Side 45
- 2.3 Right Side and Base Panel 46
- 2.4 Back 47
- 2.5.1 Display Panel 48
- 2.5.2 Keypad 50
- Preparation 53
- 3.1 Cautions on Operation 54
- 3.2 Turning the Power ON/OFF 55
- 3. Preparation 56
- RF-20AXS V*.** 57
- Basic Operation 59
- ∗ : RF-20Axs only 63
- When a Recorder Is Used: 65
- EX200n m EM30 0nm 66
- X e 1000.00 66
- PARAMETER 72
- RESPON S E5 73
- Input 0 - 1 0 73
- 1:x1 2:x 43: x16 75
- Input 0 - 3,8 85
- EX200n m EM3 00nm 87
- X e:c h 1 1000.00 87
- 10.0 sec 93
- 4.2.8 Setting Sensitivity 96
- 1:HI 2:M ED 3:LOW 97
- 0:OFF, 4-40 99
- 4. Basic Operation 100
- Application Operation 101
- Types of Screen and Their 102
- Explanations 102
- 5. Application Operation 104
- Press to 105
- Control settings group 105
- Monitor display group 107
- 5.1.3 VP Function Screen 108
- Validation support group 109
- CBM PARAMETER 111
- Enter to Select 111
- CHANGE PASSWORD 111
- Enter to Change 111
- Parameter Settings Group 113
- Control Settings Group 113
- System Settings Group 114
- Monitor Display Group 114
- RESPONSE 5 118
- Input 0 - 10 118
- 1:HI 2:MED 3:LOW 119
- 1:x1 2:x4 3:x16 119
- ANALOG1 MODE 0 120
- Input 0 - 1 120
- Input 0 - 1,8 120
- ANALOG2 MODE 0 121
- ANA1 REC RANG 1 122
- Input 0 - 9 122
- ANA2 REC RANG 1 123
- BL OFS ANA1 0 124
- Input -2 - 250mV 124
- BL OFS ANA2 0 124
- 0,1,2 or 12 125
- MARK SETTING 125
- Input 0 - 3 125
- 5.2.4 Control Settings Group 126
- EM SCAN 200-900 127
- Input 200 - 900 127
- Input 0,200-900 127
- 5.2.5 System Settings Group 129
- BRIGHTNESS 3 130
- Input 1 - 4 130
- EXT-S 0 130
- Input 0 - 5 130
- SMPL EN 873 132
- REF EN 1211 132
- Xe TIME 2000.0 132
- Set temperature 133
- Current temperature 133
- 5.3 Setting the VP Functions 134
- Validation Support Group 135
- Calibration Support Group 135
- Time [Xe LAMP USED TM] 138
- ERROR LOG 140
- Enter to Display 140
- LOG 1 08-05-12 140
- ERR LEAK DETECT 140
- No more Logs 140
- Entering the Date [DATE] 141
- Entering the Time [TIME] 141
- OP MODE 0 146
- 0:20A 1:XL 146
- INITIALIZE PARAM 146
- Enter to Init 146
- [INTERFACE] 150
- ETHERNET SPEED 0 151
- Input 0, 1-4 151
- USE GATEWAY 0 151
- 0:NO 1:GW 2:DHCP 151
- TRS MODE 3 153
- Input 0, 1-19 153
- 5.4 Creating Time Programs 154
- 5.4 Creating Time Programs 155
- Setting multiple steps: 158
- 30.00 LOOP 3 159
- Input 0 - 255 159
- 5.00 SCAN 2 159
- Input 0 - 2 159
- 5.4.5 Starting a Time Program 160
- Outputting Spectrum Data 162
- 5.5.3 Setting the Scan Type 163
- EX SCAN 200-900 164
- Input 0,2 0 0-900 165
- 5.5.6 Setting the Scan Speed 166
- SCAN SPEED 2 166
- Input 1 - 4 166
- 5.5.7 Setting Sensitivity 167
- 5.5.8 Setting Gain 168
- CELL TEMP 0 169
- 0:OFF, 4 - 40 169
- EX200nm EM300nm 170
- Xe 1000.00 170
- Enter to Select 170
- SCAN FILE 0 171
- 0:BG 1:S1 2:S2 171
- 5.5.11 Measuring Procedure 172
- SPC PLOT 174
- PLOTTIING 174
- Connecting to a CBM-20A or 175
- CBM-20Alite System Controller 175
- Controller 176
- 5.7.3 Notes on Operation 177
- XL Compatibility Mode 177
- VP function 180
- Terminals 181
- 5.8.2 Wiring 182
- EVENT 1 183
- 0,1,2 or 12 183
- Optional Cell 184
- Troubleshooting 185
- 6. Troubleshooting 186
- Dealing with Error Messages 189
- ERR EX HOME POS 190
- ERR EM HOME POS 190
- ERR EEPROM WRITE 190
- SYSTEM ERROR 190
- ERR COOLER 190
- ERR HEATER 191
- ERR OVER HEAT 191
- ERR LEAK SENS 191
- ERR LEAK SENS2 191
- NOT PROTECTED 192
- ERR Xe LAMP 192
- ERR Hg LAMP 193
- CHECK NG1 193
- CHECK NG2(EX***) 193
- CHECK NG3(EM***) 193
- ERR CELL TEMP 194
- LAMP COVER OPEN 194
- ERR PELTIER FAN 194
- ERR FAN STOP 195
- CBM-20A ERROR 195
- DATA NOT EXIST 195
- NO PEAKS 1 196
- NO PEAKS 2 196
- NO PEAKS 3 196
- ERR FILE TYPE 197
- LAMP NOT LIT 197
- SENSOR NO GOOD 197
- SELECT Xe SINGLE 197
- LOW SET TEMP 198
- CLOSED KEY 198
- NO CAL DATA 198
- NOT LOCAL MODE 198
- Hardware Validation 199
- 7.1.1 Hardware Validation 200
- Implementation of Hardware 201
- Validation 201
- 7.3 Precautions on Validation 202
- Testing Equipment 203
- Hardware Testing Equipment 204
- 7.5 Detector Validation 205
- Objective 206
- Check Procedure 206
- 7. Hardware Validation 210
- 7.5 Detector Validation 211
- When LCsolution is used: 213
- VALIDATION 214
- Press func or VP 214
- DATE YY-MM-DD 214
- 00-00-00 214
- S/N CHECK 221
- Enter to Start 221
- S/N CHECK ENTER 222
- 350/***nm1000.00 224
- TIME=***s 224
- F:** S/N:**** 224
- S/N ≥ 600 (RF-20A) 225
- 1000 (RF-20Axs) 225
- 0:Remote 1:Local 226
- NO PEAK * 228
- S/N ≥ 1000 (RF-20Axs) 230
- LEAK SENSOR TEST 232
- CHECK GOOD 232
- 7.6 System Validation 233
- 7.6 System Validation 235
- EX360nm EM450nm 237
- 7.7 If Validation Fails 244
- 7.8 Reference Information 245
- 7.8 Reference Information 247
- Maintenance 251
- 8. Maintenance 254
- 8.2.1 Inspecting the Cell 255
- Inspecting the Cell 256
- Fitting the Flow Cell Unit 257
- Parts used 258
- Simple Cleaning of the Cell 259
- Cleaning/Replacing Each Part 261
- Fig. 8.14 263
- 8.3.2 Cleaning the Cell 267
- Fitting the Cell 268
- For the RF-20A: 270
- Fitting the Emission Lens 270
- Fitting the Emission Mirror 273
- Fig. 8.35 275
- Check After Assembly 277
- 8.5 Replacing the Fuse 285
- 8.6 Replacing the Filter 287
- Wavelength calibration 289
- Wavelength accuracy check 289
- For the RF-20Axs: 290
- EX or EM 295
- Wavelength 295
- WAVE CALIB 296
- 8.8 Cleaning the Exterior 298
- Technical Information 299
- 9.1 Installation 300
- Stacking Brackets 303
- 9.1 Installation 307
- Cutting SUS tubing: 307
- Cutting resin tubing: 307
- Protective Plugs 310
- Bending Tubing for Plumbing 310
- 9. Technical Information 314
- Plumbing the Cell Outlet Tube 314
- Lowest unit: 316
- Second unit from bottom: 317
- Front Cover Installation 319
- 9.1.7 Flow Line Plumbing 321
- Connecting to a Chromatopac 329
- Connecting to a Recorder 330
- 9.2 Specifications 338
- 9.2 Specifications 339
- 9.3 Maintenance Parts 340
- Flow Cell/Plumbing Parts 341
- Electrical Parts 342
- Others 342
- Mobile Phase Characteristics 346
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